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Experimental Parameters Affecting Stripping of Rare Earth Elements from Loaded Sorptive Media in Simulated Geothermal Brines
Experimental results from several studies exploring the impact of pH and acid volume on the stripping of rare earth elements (REEs) loaded onto ligand-based media via an active column. The REEs in this experiment were loaded onto the media through exposure to a simulated geother...
Stull, D. Tusaar Corp.
May 24, 2016
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Repetitive Regeneration of Media 1 after REE Sorption from Brine 1 at 70C
This dataset shows the ability of media #1 to be loaded with REE's, stripped of the REE's sequestered, regenerated, and reused over many cycles.
Garland, G. Tusaar Corp.
Jul 23, 2015
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REE Sorption Study of Seived 50 +100 Mesh Fraction of Media 1 in Brine 1 at Different Concentrations of REE at 70C
This dataset shows the sorption capacities of smaller grain size (-50 +100 mesh) of media #1 in brine #1 at different starting concentrations of REE's at elevated temperature of 70C. The experimental conditions are 2g of 50 +100 mesh media #1 to 150mL of REE solution at concentrat...
Garland, G. Tusaar Corp.
Jun 29, 2015
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Shaker Table Experiments with Rare Earth Elements Sorption from Geothermal Brine
This dataset described shaker table experiments ran with sieved 50 +100 mesh media #1 in brine #1 that have 2ppm each of the 7 REE metals at different starting pH's of 3.5, 4.5, and 5.5. The experimental conditions are 2g media to 150mL of REE solution, at 70C.
Garland, G. Tusaar Corp.
Jul 21, 2015
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Comparison of Rare Earth Element Sorption Between Fresh and Partially Loaded Media Using Simulated Geothermal Brine
A study comparing the REE sorption characteristics of fresh ligand-based sorption media and media partially loaded with REEs when exposed to a simulated geothermal brine with known mineral concentrations, REE7. Sorption rates were tested using microcosm shaker tests. Results sugg...
Stull, D. Tusaar Corp.
May 24, 2016
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Dynamic Column Extraction for Europium on Media 1 at Ambient Temperature
This is a dataset for a 200ppm europium solution sent through a column with 12g of media #1 at pH of 3.2. This column experiment was run at ambient temperature at a flow rate of 2mL/min.
Garland, G. Tusaar Corp.
Apr 07, 2015
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Protocol for Regeneration of Ligand-Depleted Adsorption Media for Rare Earth Element Recovery from Geothermal Brine
Description of experimental protocol used to characterize the effectiveness of regenerating ligand-based adsorption media through the addition of ligands when media were previously depleted of ligands during use. Results of the effectiveness of this regeneration are also described.
Stull, D. Tusaar Corp.
May 24, 2016
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Method to Recover Media Ligand Losses During Sorption of Rare Earth Elements from Simulated Geothermal Brines
This document describes the method and results of an in-situ experiment used to confirm that ligand bleed from a sorptive media can be contained. The experiment focused on maintaining the media's sorption of rare earth elements (REE) obtained from a simulated geothermal brine dop...
Stull, D. Tusaar Corp.
May 24, 2016
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Rare Earth Desorption Test with Citrate and Bicarbonate
LBT (lanthanide binding tag) cells were grown overnight in LB media with 0.05% Amp. 1:100 subculture taken from overnights, grown for 2 hours. LBT was induced with 0.002% arabinose added for 3 hours. REE adsorption was done by combining 350 ul (0.25% 1M MES, 12.5 uM Tb, and 12.5 u...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jun 01, 2017
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In-Situ Process for Sorption and Stripping of Rare Earth Elements from Simulated Geothermal Brine
Description of a conceptual commercial process to remove rare earth elements (REEs) from geothermal brine, based on a small-scale laboratory experiment to load, strip, and regenerate a ligand-based media used to adsorb REEs from a simulated brine doped with known mineral concentra...
Stull, D. Tusaar Corp.
May 24, 2016
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Techno-Economic Assessment for Integrating Biosorption into Rare Earth Recovery Process
The current uncertainty in the global supply of rare earth elements (REEs) necessitates the development of novel extraction technologies that utilize a variety of REE source materials. Herein, we examined the techno-economic performance of integrating a biosorption approach into ...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jul 01, 2017
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Great Salt Lake Composition and Rare Earth Speciation Analysis
We have conducted aqueous speciation analyses of the Great Salt Lake (GSL) brine sample (Table 1) and a mock geo sample (Table 2) spiked with 1 ppb Tb and 100 ppb Tb. The GSL speciation (Figure 1) aligns with our basic speciation expectations that strong carbonate complexes would ...
Jiao, Y. et al Lawrence Livermore National Laboratory
Apr 19, 2017
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