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Magnetic Nanofluid Rare Earth Element Extraction Process Report, Techno Economic Analysis, and Results for Geothermal Fluids

This GDR submission is an interim technical report and raw data files from the first year of testing on functionalized nanoparticles for rare earth element extraction from geothermal fluids. The report contains Rare Earth Element uptake results (percent removal, mg Rare Earth Ele...
McGrail, P. Pacific Northwest National Laboratory
Mar 14, 2016
3 Resources
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Shaker Test Results Comparing Rare Earth Element Sorption Between Natural and Doped Simulated Geothermal Brine

Shaker test data comparing rare earth element (REE) sorption onto Tusaar media between one natural geothermal brine and two simulated brines doped with known mineral concentrations.
Stull, D. Tusaar Corp.
May 24, 2016
1 Resources
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Technical Report-Rare Earth Element Concentrations in Wyoming's Produced Waters

This study is a joint effort by the University of Wyoming (UW), the UW Engineering Department (UW-ENG), and Idaho National Laboratories (INL) and the United States Geological Survey (USGS) to describe rare earth element concentrations in oil and gas produced waters. In this work w...
Quillinan, S. et al University of Wyoming
Jul 01, 2017
2 Resources
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Rare Earth Element Concentrations in Wyoming's Produced Waters

Version 2. This study is a joint effort by the University of Wyoming (UW), the UW Engineering Department (UW-ENG), and Idaho National Laboratories (INL) and the United States Geological Survey (USGS) to describe rare earth element concentrations in oil and gas produced waters. In ...
Quillinan, S. et al University of Wyoming
Jul 01, 2017
1 Resources
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Technical Report-Rare Earth Element Data Associated with Oil and Gas Reservoir Rock

This work was developed to complement the geochemical assessments of produced water and geothermal water samples. Specifically, this task was designed to test the influence of reservoir rock-type and corresponding mineralogy/geochemistry on the concentrations of REE found in oil a...
McLaughlin, J. et al University of Wyoming
Jul 01, 2017
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Aqueous Rare Earth Element Patterns and Concentration in Thermal Brines Associated with Oill and Gas Production

This study is part of a joint effort by the University of Wyoming (UW) School of Energy Resources (SER), the UW Engineering Department, Idaho National Laboratories (INL), and the United States Geological Survey (USGS) to describe rare earth element concentrations in oil and gas pr...
Nye, C. et al University of Wyoming
Feb 01, 2017
2 Resources
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Column Sorption Uptake and Regeneration Study; Rare Earth Element Sorbent Uptake and Sorbent Stripping

Study of rare earth element (REE) uptake from geothermal brine simulant by column loading, metal recovery through stripping, and regeneration of column for re-loading. Simulated brine testing.
Lanyk, T. Tusaar Corp.
Dec 18, 2015
3 Resources
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Experimental Parameters Affecting Stripping of Rare Earth Elements from Loaded Sorptive Media in Simulated Geothermal Brines

Experimental results from several studies exploring the impact of pH and acid volume on the stripping of rare earth elements (REEs) loaded onto ligand-based media via an active column. The REEs in this experiment were loaded onto the media through exposure to a simulated geother...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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Method to Recover Media Ligand Losses During Sorption of Rare Earth Elements from Simulated Geothermal Brines

This document describes the method and results of an in-situ experiment used to confirm that ligand bleed from a sorptive media can be contained. The experiment focused on maintaining the media's sorption of rare earth elements (REE) obtained from a simulated geothermal brine dop...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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Recovery of Rare Earths, Precious Metals and Other Critical Materials from Geothermal Waters with Advanced Sorbent Structures

The work evaluates, develops and demonstrates flexible, scalable mineral extraction technology for geothermal brines based upon solid phase sorbent materials with a specific focus upon rare earth elements (REEs). The selected organic and inorganic sorbent materials demonstrated h...
Addleman, R. et al Pacific Northwest National Laboratory
Sep 30, 2015
2 Resources
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Protocol for Regeneration of Ligand-Depleted Adsorption Media for Rare Earth Element Recovery from Geothermal Brine

Description of experimental protocol used to characterize the effectiveness of regenerating ligand-based adsorption media through the addition of ligands when media were previously depleted of ligands during use. Results of the effectiveness of this regeneration are also described.
Stull, D. Tusaar Corp.
May 24, 2016
1 Resources
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Comparison of Rare Earth Element Sorption Between Fresh and Partially Loaded Media Using Simulated Geothermal Brine

A study comparing the REE sorption characteristics of fresh ligand-based sorption media and media partially loaded with REEs when exposed to a simulated geothermal brine with known mineral concentrations, REE7. Sorption rates were tested using microcosm shaker tests. Results sugg...
Stull, D. Tusaar Corp.
May 24, 2016
1 Resources
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Raft River Geothermal Field Well Head Brine Sample

Raw data and data workup of assay for real-world brine sample. Brine sample was taken at the well head.
Lanyk, T. Tusaar Corp.
Dec 18, 2015
2 Resources
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Improved Rare Earth Element Sorption from Simulated Geothermal Brines: Effect of Gassed versus Degassed Brines

A study exploring sorption and stripping characteristics of sorption media when simulated geothermal brines are degassed or not degassed. Experiments were done at 70degC. The brines used in this study were formulated by Tusaar. The two brines used/simulated are labeled 1M and 1C...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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REE Adsorption Performance with Immobilized Caulobacter Biofilms

This submission includes data collected from experiments on the performance of rare earth adsorption by immobilized bacteria that accompany the FY18 Q2 and Q3 quarter reports. Relevant information from these reports is included in a resource below. The spreadsheet below includes d...
Jiao, Y. and Park, D. Lawrence Livermore National Laboratory
Apr 01, 2018
2 Resources
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Rare Earth Element Sorption Study on sieved 50 +100 mesh fraction of Media 1 in Brine 1 with Different Starting pHs at 70C

This is a continuation of the rare earth element sorption study for shaker bath tests on 2g media #1 in 150mL brine #1 with different starting pH's at 70C. In a previous submission we reported data for shaker bath tests for brine #1 with starting pH's of 3.5, 4.5 and 5.5. In this ...
Garland, G. Tusaar Corp.
Sep 29, 2015
5 Resources
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Dynamic Column Extraction for Europium on Media 1 at Ambient Temperature

This is a dataset for a 200ppm europium solution sent through a column with 12g of media #1 at pH of 3.2. This column experiment was run at ambient temperature at a flow rate of 2mL/min.
Garland, G. Tusaar Corp.
Apr 07, 2015
2 Resources
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Assessing REE Concentrations in Geothermal and Oil and Gas Produced Waters: A Potential Domestic Source of Strategic Mineral Commodities

The project team collected and analyzed 224 water samples and 101 matching rock samples. INL's improved method of measuring aqueous REEs allows study of samples previously thought too volume limited to measure. The study found that aqueous REEs occur at trace levels in all analyz...
Quillinan, S. et al University of Wyoming
Mar 08, 2019
1 Resources
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Repetitive Regeneration of Media 1 after REE Sorption from Brine 1 at 70C

This dataset shows the ability of media #1 to be loaded with REE's, stripped of the REE's sequestered, regenerated, and reused over many cycles.
Garland, G. Tusaar Corp.
Jul 23, 2015
3 Resources
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In-Situ Process for Sorption and Stripping of Rare Earth Elements from Simulated Geothermal Brine

Description of a conceptual commercial process to remove rare earth elements (REEs) from geothermal brine, based on a small-scale laboratory experiment to load, strip, and regenerate a ligand-based media used to adsorb REEs from a simulated brine doped with known mineral concentra...
Stull, D. Tusaar Corp.
May 24, 2016
1 Resources
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Techno-Economic Assessment for Integrating Biosorption into Rare Earth Recovery Process

The current uncertainty in the global supply of rare earth elements (REEs) necessitates the development of novel extraction technologies that utilize a variety of REE source materials. Herein, we examined the techno-economic performance of integrating a biosorption approach into a...
Jiao, Y. et al Lawrence Livermore National Laboratory
Oct 09, 2017
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Core-Shell REE Sorbent Extraction Data

Solution chemical analysis data for magnetic core shell sorbent materials. Deionized water and brine solutions were spiked with five rare earth elements and the solutions analyzed after approximately 5 minutes exposure to the sorbent particles.
Thallapally, P. Pacific Northwest National Laboratory
Apr 27, 2017
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Surface Complexation Modeling of Terbium Biosorption onto E. Coli Bacterial Surfaces with Lanthanide Binding Tags

Lanthanide binding tags (LBTs) have been engineered onto native Escherichia coli (E. coli) bacterial surfaces to enhance extraction and recovery of rare earth elements (REEs). Three strains of E. coli were studied: (1) the native E. coli surface, (2) a mutant E. coli surface with ...
Jiao, Y. Lawrence Livermore National Laboratory
Apr 01, 2018
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Recovery of Rare Earth Elements from Geothermal Fluids through Bacterial Cell Surface Adsorption

We summarized the FY17 and part of FY18 results of the analysis of the effect of several parameters (e.g., total dissolved solids, specific competing metals, pH, and temperature) on REE recovery from geothermal brine in a manuscript that was submitted to Environmental Science & Te...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jan 01, 2018
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Advanced Sorbent Structure Recovery of Rare Earths, Precious Metals and Other Critical Materials from Geothermal Waters and Its Associated Technoeconomics

The work evaluates, develops and demonstrates flexible, scalable mineral extraction technology for geothermal brines based upon solid phase sorbent materials with a specific focus upon rare earth elements (REEs). The selected organic and inorganic sorbent materials (silica and MOF...
Addleman, R. et al Pacific Northwest National Laboratory
Sep 21, 2016
1 Resources
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