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Protocol for Regeneration of Ligand-Depleted Adsorption Media for Rare Earth Element Recovery from Geothermal Brine
Description of experimental protocol used to characterize the effectiveness of regenerating ligand-based adsorption media through the addition of ligands when media were previously depleted of ligands during use. Results of the effectiveness of this regeneration are also described.
Stull, D. Tusaar Corp.
May 24, 2016
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Compilation of Rare Earth Element Analyses from US Geothermal Fields and Mid Ocean Ridge Hydrothermal Vents
Compilation of rare earth element and associated major and minor dissolved constituent analytical data for USA geothermal fields and global seafloor hydrothermal vents. Data is in original units. Reference to and use of this data should be attributed to the original authors and pu...
Fowler, A. University of California
Oct 01, 2015
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Aqueous Rare Earth Elements, Concentration, and Stable Isotopes in Deep Basin Brines, Wyoming
Presentation given to National Groundwater Association meeting on deep basin brines. This presentation discusses why produced waters are being observed, the importance of REE's, the study areas examined, the data collected, and the relationship between REE concentration and possib...
Quillinan, S. et al University of Wyoming
Apr 25, 2017
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Chelating Resins for Selective Separation and Recovery of Rare Earth Elements from Low Temperature Geothermal Water
Study on the use of organic ligands to extract lanthanides from low temperature geothermal water.
Callura, J. Carnegie Mellon University
Dec 31, 2016
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Comparison of Rare Earth Element Sorption Between Fresh and Partially Loaded Media Using Simulated Geothermal Brine
A study comparing the REE sorption characteristics of fresh ligand-based sorption media and media partially loaded with REEs when exposed to a simulated geothermal brine with known mineral concentrations, REE7. Sorption rates were tested using microcosm shaker tests. Results sugg...
Stull, D. Tusaar Corp.
May 24, 2016
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Raft River Geothermal Field Well Head Brine Sample
Raw data and data workup of assay for real-world brine sample. Brine sample was taken at the well head.
Lanyk, T. Tusaar Corp.
Dec 18, 2015
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Improved Rare Earth Element Sorption from Simulated Geothermal Brines: Effect of Gassed versus Degassed Brines
A study exploring sorption and stripping characteristics of sorption media when simulated geothermal brines are degassed or not degassed. Experiments were done at 70degC. The brines used in this study were formulated by Tusaar. The two brines used/simulated are labeled 1M and 1C...
Stull, D. Tusaar Corp.
May 24, 2016
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Magnetic Test Loop Particle Retention Data for REE Extraction from Geothermal Fluids
Measurements of particle extraction efficiency under various flow rate and magnetic power conditions
McGrail, P. and Liu, J. Pacific Northwest National Laboratory
Jul 27, 2018
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REE Adsorption Performance with Immobilized Caulobacter Biofilms
This submission includes data collected from experiments on the performance of rare earth adsorption by immobilized bacteria that accompany the FY18 Q2 and Q3 quarter reports. Relevant information from these reports is included in a resource below. The spreadsheet below includes d...
Jiao, Y. and Park, D. Lawrence Livermore National Laboratory
Apr 01, 2018
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Great Salt Lake Composition and Rare Earth Speciation Analysis
We have conducted aqueous speciation analyses of the Great Salt Lake (GSL) brine sample (Table 1) and a mock geo sample (Table 2) spiked with 1 ppb Tb and 100 ppb Tb. The GSL speciation (Figure 1) aligns with our basic speciation expectations that strong carbonate complexes would ...
Jiao, Y. et al Lawrence Livermore National Laboratory
Apr 19, 2017
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Brine Geochemistry from Soda Geyser, Idaho
These brine samples are collected from the Soda Geyser (a thermal feature, temperature ~30 C) in Soda Springs, Idaho. These samples also represent the overthrust brines typical of oil and gas plays in western Wyoming. Samples were collected from the source and along the flow chan...
Neupane, G. and McLing, T. University of Wyoming
Apr 01, 2017
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Rare Earth Element Sorption Study on sieved 50 +100 mesh fraction of Media 1 in Brine 1 with Different Starting pHs at 70C
This is a continuation of the rare earth element sorption study for shaker bath tests on 2g media #1 in 150mL brine #1 with different starting pH's at 70C. In a previous submission we reported data for shaker bath tests for brine #1 with starting pH's of 3.5, 4.5 and 5.5. In this ...
Garland, G. Tusaar Corp.
Sep 29, 2015
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Dynamic Column Extraction for Europium on Media 1 at Ambient Temperature
This is a dataset for a 200ppm europium solution sent through a column with 12g of media #1 at pH of 3.2. This column experiment was run at ambient temperature at a flow rate of 2mL/min.
Garland, G. Tusaar Corp.
Apr 07, 2015
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Assessing REE Concentrations in Geothermal and Oil and Gas Produced Waters: A Potential Domestic Source of Strategic Mineral Commodities
The project team collected and analyzed 224 water samples and 101 matching rock samples. INL's improved method of measuring aqueous REEs allows study of samples previously thought too volume limited to measure.
The study found that aqueous REEs occur at trace levels in all analyz...
Quillinan, S. et al University of Wyoming
Mar 08, 2019
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Repetitive Regeneration of Media 1 after REE Sorption from Brine 1 at 70C
This dataset shows the ability of media #1 to be loaded with REE's, stripped of the REE's sequestered, regenerated, and reused over many cycles.
Garland, G. Tusaar Corp.
Jul 23, 2015
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In-Situ Process for Sorption and Stripping of Rare Earth Elements from Simulated Geothermal Brine
Description of a conceptual commercial process to remove rare earth elements (REEs) from geothermal brine, based on a small-scale laboratory experiment to load, strip, and regenerate a ligand-based media used to adsorb REEs from a simulated brine doped with known mineral concentra...
Stull, D. Tusaar Corp.
May 24, 2016
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Techno-Economic Assessment for Integrating Biosorption into Rare Earth Recovery Process
The current uncertainty in the global supply of rare earth elements (REEs) necessitates the development of novel extraction technologies that utilize a variety of REE source materials. Herein, we examined the techno-economic performance of integrating a biosorption approach into a...
Jiao, Y. et al Lawrence Livermore National Laboratory
Oct 09, 2017
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Techno-Economic Assessment for Integrating Biosorption into Rare Earth Recovery Process
The current uncertainty in the global supply of rare earth elements (REEs) necessitates the development of novel extraction technologies that utilize a variety of REE source materials. Herein, we examined the techno-economic performance of integrating a biosorption approach into ...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jul 01, 2017
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Core-Shell REE Sorbent Extraction Data
Solution chemical analysis data for magnetic core shell sorbent materials. Deionized water and brine solutions were spiked with five rare earth elements and the solutions analyzed after approximately 5 minutes exposure to the sorbent particles.
Thallapally, P. Pacific Northwest National Laboratory
Apr 27, 2017
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Rare Earth Desorption Test with Citrate and Bicarbonate
LBT (lanthanide binding tag) cells were grown overnight in LB media with 0.05% Amp. 1:100 subculture taken from overnights, grown for 2 hours. LBT was induced with 0.002% arabinose added for 3 hours. REE adsorption was done by combining 350 ul (0.25% 1M MES, 12.5 uM Tb, and 12.5 u...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jun 01, 2017
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Surface Complexation Modeling of Terbium Biosorption onto E. Coli Bacterial Surfaces with Lanthanide Binding Tags
Lanthanide binding tags (LBTs) have been engineered onto native Escherichia coli (E. coli) bacterial surfaces to enhance extraction and recovery of rare earth elements (REEs). Three strains of E. coli were studied: (1) the native E. coli surface, (2) a mutant E. coli surface with ...
Jiao, Y. Lawrence Livermore National Laboratory
Apr 01, 2018
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Rare Earth Adsorption and Desorption with PEGDA Beads
We synthesized PEGDA polymer hydrogel beads for cell embedding and compared REE biosorption with these beads via a gravity-driven flow through setup. One way to set up a flow through system is by cell encapsulation into polymer beads with a column setup similar to that used in th...
Jiao, Y. et al Lawrence Livermore National Laboratory
Mar 01, 2017
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Recovery of Rare Earth Elements from Geothermal Fluids through Bacterial Cell Surface Adsorption
We summarized the FY17 and part of FY18 results of the analysis of the effect of several parameters (e.g., total dissolved solids, specific competing metals, pH, and temperature) on REE recovery from geothermal brine in a manuscript that was submitted to Environmental Science & Te...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jan 01, 2018
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RN12 and RN30 Epidote anlayses
Results for laser ablation measurement of rare earth elements and electron microprobe analysis of major elements in hydrothermal epidote. Laser ablation measurements were completed using an Agilent 7700 quadrupole ICP-MS coupled with 193nm Photon Instruments Excimer laser.
Fowler, A. and Zierenberg, R. University of California
Jan 01, 2015
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Advanced Sorbent Structure Recovery of Rare Earths, Precious Metals and Other Critical Materials from Geothermal Waters and Its Associated Technoeconomics
The work evaluates, develops and demonstrates flexible, scalable mineral extraction technology for geothermal brines based upon solid phase sorbent materials with a specific focus upon rare earth elements (REEs). The selected organic and inorganic sorbent materials (silica and MOF...
Addleman, R. et al Pacific Northwest National Laboratory
Sep 21, 2016
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